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Cited article:

Dehydration of Cu−Hectorite:  Water Isotherm, XRD, and EPR Studies

Faïza Annabi-Bergaya, Henriette Estrade-Szwarckopf and Henri Van Damme
The Journal of Physical Chemistry 100 (10) 4120 (1996)
https://doi.org/10.1021/jp950283v